C₂₀H₃₆O₄SSi

Base Information

Chemical Name:C₂₀H₃₆O₄SSi
CAS No.:912293-10-8
Molecular Formula:C₂₀H₃₆O₄SSi
Molecular Weight:400.655
Hs Code.:

C<sub>20</sub>H<sub>36</sub>O<sub>4</sub>SSi

Synonyms:C₂₀H₃₆O₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₃₆O₄SSi

Chemical Property:

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Technology Process of C₂₀H₃₆O₄SSi

There total 6 articles about C₂₀H₃₆O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 912293-19-7
C₁₃H₃₀O₂Si

: 98-59-9
p-toluenesulfonyl chloride

: 912293-10-8
C₂₀H₃₆O₄SSi

Guidance literature:: In pyridine; at 0 - 20 ℃; for 16h;
DOI:10.1055/s-2006-942459

Reference yield:

: 912293-09-5
C₁₄H₃₀O₃Si

: 912293-10-8
C₂₀H₃₆O₄SSi

Guidance literature:: Multi-step reaction with 2 steps

1: 6.31 g / DIBAL-H / tetrahydrofuran; toluene / 2.5 h / -78 °C

2: 97 percent / pyridine / 16 h / 0 - 20 °C

With diisobutylaluminium hydride; In tetrahydrofuran; pyridine; toluene;
DOI:10.1055/s-2006-942459

Reference yield:

: 19013-37-7
dimethyl 3-methylglutarate

: 912293-10-8
C₂₀H₃₆O₄SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: 95 percent / porcine liver esteraze / methanol; various solvent(s) / pH 7

2.1: 80 percent / BH₃*SMe₂ / tetrahydrofuran

3.1: 90 percent / imidazole / dimethylformamide

4.1: LDA; n-BuLi / tetrahydrofuran; hexane / 2 h / -78 °C

4.2: tetrahydrofuran; hexane / 1.33 h / -78 - 20 °C

5.1: 6.31 g / DIBAL-H / tetrahydrofuran; toluene / 2.5 h / -78 °C

6.1: 97 percent / pyridine / 16 h / 0 - 20 °C

With 1H-imidazole; n-butyllithium; dimethylsulfide borane complex; porcine liver esteraze; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; pyridine; methanol; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-2006-942459