1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

Base Information

Chemical Name:1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol
CAS No.:81713-00-0
Molecular Formula:C₃₆H₄₀O₁₁S₂
Molecular Weight:712.839
Hs Code.:

Synonyms:1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

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Chemical Property of 1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

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Technology Process of 1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

There total 1 articles about 1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 80971-15-9
1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-chiro-inositol

: 98-59-9
p-toluenesulfonyl chloride

: 81713-00-0
1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With pyridine; at 60 ℃; for 12h;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield: 96.0%

: 81713-00-0
1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

: 81713-02-2
1L-1,7-Anhydro-3,4-di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With sodium methylate; In methanol; for 0.75h; Ambient temperature;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81713-00-0
1L-3,4-Di-O-benzyl-1-C-hydroxymethyl-2-O-methyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

: 1D-(1N,2,4/3)-1-Azido-5-C-azidomethyl-2,3-di-O-benzyl-4-O-methyl-2,3,4-trihydroxycyclohex-5-en

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / sodium methoxide / methanol / 0.75 h / Ambient temperature

2: 87 percent / 3-methyl-2-selenoxobenzothiazol, trifluoroacetic acid / CH₂Cl₂ / 20 h / Ambient temperature

3: 92 percent / pyridine / 2 h / 20 °C

4: 82 percent / sodium azide / dimethylformamide / 1 h / 80 °C

With pyridine; sodium azide; N-methyl-1,3-benzothiazole-2(3H)-selone; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)88052-0