(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

Base Information

Chemical Name:(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride
CAS No.:25126-04-9
Molecular Formula:C₂₀H₂₅N₃O₃*ClH
Molecular Weight:391.898
Hs Code.:

Synonyms:(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

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Chemical Property of (S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

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Technology Process of (S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

There total 1 articles about (S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 25126-45-8
(S)-benzyl 6-( tert-butoxycarbonylamino)-1-oxo-1-(phenylamino)hexan-2-ylcarbamate

: 25126-04-9
(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; Cooling with ice;

Reference yield: 89.0%

: 25126-04-9
(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

: 993-12-4
dimethylphosphinothioic chloride

: 1245943-01-4
(S)-benzyl 6-(dimethylphosphorothioylamino)-1-oxo-1-(phenylamino)hexan-2-ylcarbamate

Guidance literature:: (S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride; With pyridine; N-ethyl-N,N-diisopropylamine; at 0 ℃; for 0.25h; Inert atmosphere;

dimethylphosphinothioic chloride; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2010.06.035

Reference yield: 86.0%

: 40052-13-9
mono-tert-butyl malonate

: 25126-04-9
(S)-5-(benzyloxycarbonylamino)-6-oxo-6-(phenylamino)hexan-1-aminium chloride

: 1159275-90-7
N-(5-benzyloxycarbonylamino-5-phenylcarbamoylpentyl)malonamic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;