3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

Base Information

Chemical Name:3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one
CAS No.:131146-40-2
Molecular Formula:C₁₇H₁₂O₆
Molecular Weight:312.279
Hs Code.:

Synonyms:3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

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Chemical Property of 3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

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Technology Process of 3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

There total 12 articles about 3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 131146-38-8
3-(3',4'-dihydroxyphenyl)-5-(4''-hydroxyphenyl)methylene-4-methoxyfuran-2(5H)-one

: 131146-40-2
3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

Guidance literature:: With lithium bromide; In N,N-dimethyl-formamide; at 150 ℃; for 0.116667h;

Reference yield: 69.0%

: 929688-03-9
(Z)-3-(3,4-dimethoxyphenyl)-4-hydroxy-5-(4-methoxybenzylidene)furan-2(5H)-one

: 131146-40-2
3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

Guidance literature:: With boron tribromide; In hexane; dichloromethane; at 20 ℃; for 8h;
DOI:10.1055/s-2007-983803

Reference yield:

: 131146-34-4
3-(3',4'-dimethoxyphenyl)-4-methoxy-5-<(4''-methoxyphenyl)methyl>furan-2(5H)-one

: 131146-40-2
3-(3',4'-dihydroxyphenyl)-4-hydroxy-5-<(4''-hydroxyphenyl)methylene>furan-2(5H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide / CCl₄ / 0.08 h / Heating; irradiation

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / benzene / 0.5 h / Ambient temperature

3: 82 percent / boron tribromide / CH₂Cl₂ / 0.5 h / Heating

4: 70 percent / LiBr / dimethylformamide / 0.12 h / 150 °C

With N-Bromosuccinimide; boron tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; benzene;