cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

Base Information

Chemical Name:cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate
CAS No.:1018811-87-4
Molecular Formula:C₂₆H₄₆N₂O₄
Molecular Weight:450.662
Hs Code.:

Synonyms:cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

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Technology Process of cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

There total 6 articles about cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 916210-80-5
trans-4-(N-tert-butoxycarbonylaminomethyl)cyclohexane carboxaldehyde

: 956928-36-2
cyclopentyl (2S)-amino(cyclohexyl)acetate hydrochloride

: 1018811-87-4
cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 16h;

Reference yield:

: 914604-31-2
(S)-tert-butoxycarbonylamino-cyclohexyl-acetic acid cyclopentyl ester

: 1018811-87-4
cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; dichloromethane / 24 h / 20 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 16 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 1074-62-0
4-(aminomethyl)-cyclohexanemethanol

: 1018811-87-4
cyclopentyl (2S)-{[(4-{[(tert-butoxycarbonyl)amino]methyl}cyclohexyl)methyl]amino}(cyclohexyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / 1,4-dioxane; water / 16 h / 20 °C

2: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -65 - 0 °C

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 16 h / 20 °C

With sodium hydroxide; oxalyl dichloride; sodium tris(acetoxy)borohydride; dimethyl sulfoxide; In 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane;