N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

Base Information

Chemical Name:N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine
CAS No.:280142-48-5
Molecular Formula:C₂₃H₃₀N₂
Molecular Weight:334.505
Hs Code.:

Synonyms:N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

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Technology Process of N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

There total 2 articles about N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 58335-10-7
3-Methyl-2-butenylzinc bromide

: 138812-17-6
N,N'-bis<(S)-1-phenylethyl>ethanediimine

: 280142-48-5
N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1055/s-2000-6377

Reference yield:

: 138812-17-6
N,N'-bis<(S)-1-phenylethyl>ethanediimine

: 870-63-3
prenyl bromide

: 280142-48-5
N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

Guidance literature:: With cerium(III) chloride; zinc; In tetrahydrofuran; at 25 ℃; for 0.5h;
DOI:10.1055/s-2002-19343

Reference yield:

: 280142-48-5
N-[1(S)-Phenylethyl]-3,3-dimethyl-2(R)-[1(S)-phenylethylamino]-4-penteneimine

: (4R,5R)-3,3,6,6-Tetramethyl-5-((S)-1-phenyl-ethylamino)-octan-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: CeCl₃*7H₂O / tetrahydrofuran / 1 h / 65 °C

2: 54 percent / tetrahydrofuran / 1 h / 25 °C

3: H₂ / 10 percent Pd/C / methanol / 6 h / 2327.17 Torr

With cerium(III) chloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1055/s-2002-19343