(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

Base Information

Chemical Name:(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide
CAS No.:326921-56-6
Molecular Formula:C₃₄H₄₈O₄Si
Molecular Weight:548.838
Hs Code.:

Synonyms:(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

Suppliers and Price of (9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

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Technology Process of (9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

There total 16 articles about (9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 326921-62-4
(9R,10E,12R,13S,15Z)-12-t-butyldimethylsilyloxy-13-t-butyldiphenylsilyloxyoctadeca-10,15-dien-9-olide

: 326921-56-6
(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

Guidance literature:: With hydrogen fluoride; In acetonitrile; at 0 - 20 ℃; for 1h;
DOI:10.1016/S0040-4020(01)00279-4

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 326921-56-6
(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 51 percent / HF / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; hydrogen fluoride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)00279-4

Reference yield:

: 326921-55-5
(9R,10E,12R,13S,15Z)-12-t-butyldimethylsilyloxy-13-hydroxyoctadeca-10,15-dien-9-olide

: 326921-56-6
(9R,10E,12R,13S,15Z)-13-t-butyldiphenylsilyloxy-12-hydroxyoctadeca-10,15-dien-9-olide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 51 percent / HF / acetonitrile / 1 h / 0 - 20 °C

With 1H-imidazole; hydrogen fluoride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)00279-4