4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL

Base Information

Chemical Name:4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL
CAS No.:1973-36-0
Molecular Formula:C₂₉H₄₉ClO₂
Molecular Weight:465.16
Hs Code.:
Mol file:1973-36-0.mol

Synonyms:5a-Cholestan-6a-ol, 3b-chloro-, acetate (7CI,8CI)

Suppliers and Price of 4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL

Chemical Property:

Melting Point:103-106 °C
Refractive Index:1.5600 (estimate)
Boiling Point:365.73°C (rough estimate)
PSA：27.96000
Density:1.0145 (rough estimate)
LogP:1.84600

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 37/39-26

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL

There total 6 articles about 4-TERT-BUTYLIMINOMETHYL-2,2,5,5-TETRAMETH YL-3-IMIDAZOLINE-1-OXYL,FREE RADICAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1251-93-0
(3S,5S,6S,8S,9S,10R,13R,14S,17R)-3-Chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-ol

: 108-24-7
acetic anhydride

: 1973-36-0
Acetic acid (3S,5S,6S,8S,9S,10R,13R,14S,17R)-3-chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-yl ester

Guidance literature:: With pyridine;

Reference yield:

: 80725-17-3
3β-chloro-(6S)-6,6-oxyethylenethio-5α-cholestane

: 1973-36-0
Acetic acid (3S,5S,6S,8S,9S,10R,13R,14S,17R)-3-chloro-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 16.6 percent / LiAlH₄, AlCl₃ / diethyl ether / Heating

2: 85 percent / pyridine

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether;