2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate

Base Information

Chemical Name:2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate
CAS No.:949449-10-9
Molecular Formula:C₁₈H₁₄O₄S
Molecular Weight:326.373
Hs Code.:
DSSTox Substance ID:DTXSID201196230

Synonyms:2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate;DTXSID201196230;949449-10-9

Suppliers and Price of 2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:326.06128010
Heavy Atom Count:23
Complexity:573

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=C=CC(=O)OC1=CC=CC=C1C=CS(=O)(=O)C2=CC=CC=C2
Isomeric SMILES:C=C=CC(=O)OC1=CC=CC=C1/C=C/S(=O)(=O)C2=CC=CC=C2

Technology Process of 2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate

There total 3 articles about 2-[(1E)-2-(Phenylsulfonyl)ethenyl]phenyl 2,3-butadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 949449-22-3
(E)-1-hydroxyl-2-(2-(phenylsulfonyl)vinyl)benzene

: 2345-51-9
3-butynoic acid

: 949449-10-9
2-[(2-benzenesulfonyl)vinyl]phenyl allenoate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃;
DOI:10.1021/ol071181d

Reference yield:

: 56069-39-7
diethyl phenylsulfonylmethylphosphonate

: 949449-10-9
2-[(2-benzenesulfonyl)vinyl]phenyl allenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaH / tetrahydrofuran / 2 h / 20 °C

2: 53 percent / 2-fluoro-1-methylpyridinium triflate; potassium carbonate / CH₂Cl₂ / 20 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol071181d

Reference yield:

: 90-02-8
salicylaldehyde

: 949449-10-9
2-[(2-benzenesulfonyl)vinyl]phenyl allenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaH / tetrahydrofuran / 2 h / 20 °C

2: 53 percent / 2-fluoro-1-methylpyridinium triflate; potassium carbonate / CH₂Cl₂ / 20 °C

With sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol071181d