2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

Base Information

Chemical Name:2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole
CAS No.:882692-40-2
Molecular Formula:C₅₁H₅₀N₂O₄
Molecular Weight:754.969
Hs Code.:

Synonyms:2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

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Chemical Property of 2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

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Technology Process of 2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

There total 1 articles about 2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 765-87-7
cyclohexane-1,2-dione

: 577995-57-4
(2R,3S,4S)-2,3,4-tris(benzyloxy)-5-(trityloxy)pentanal

: 882692-40-2
2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

Guidance literature:: With ammonia; In methanol; water; at 70 ℃; for 1h;
DOI:10.1002/ejoc.200500414

Reference yield:

: 882692-40-2
2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

: 882692-44-6
(2S,3S,4S)-2,3,4-tris(benzyloxy)-1,2,3,4,6,7,8,9-octahydrobenz[4,5]imidazo[1,2-a]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / HCl / dioxane / 2 h / 80 °C

2: pyridine / 0.17 h / 0 °C

3: 270 mg / pyridine / 2 h / 80 °C

With pyridine; hydrogenchloride; In 1,4-dioxane; pyridine;
DOI:10.1002/ejoc.200500414

Reference yield:

: 882692-40-2
2-[(1S,2R,3S)-1,2,3-tris(benzyloxy)-4-(trityloxy)butyl]-4,5,6,7-tetrahydro-1Y-benzimidazole

: Methanesulfonic acid (2S,3R,4S)-2,3,4-tris-benzyloxy-4-(4,5,6,7-tetrahydro-1H-benzoimidazol-2-yl)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / HCl / dioxane / 2 h / 80 °C

2: pyridine / 0.17 h / 0 °C

With pyridine; hydrogenchloride; In 1,4-dioxane;
DOI:10.1002/ejoc.200500414