Benzenemethanol, alpha-cyclohexylidene-, 1-acetate

Base Information

Chemical Name:Benzenemethanol, alpha-cyclohexylidene-, 1-acetate
CAS No.:34701-37-6
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:
DSSTox Substance ID:DTXSID901248000
Nikkaji Number:J2.006.357B

Synonyms:DTXSID901248000;34701-37-6;Benzenemethanol, alpha-cyclohexylidene-, 1-acetate

Suppliers and Price of Benzenemethanol, alpha-cyclohexylidene-, 1-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, alpha-cyclohexylidene-, 1-acetate

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:230.130679813
Heavy Atom Count:17
Complexity:290

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC(=C1CCCCC1)C2=CC=CC=C2

Technology Process of Benzenemethanol, alpha-cyclohexylidene-, 1-acetate

There total 2 articles about Benzenemethanol, alpha-cyclohexylidene-, 1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 108-22-5
Isopropenyl acetate

: 712-50-5
Cyclohexyl phenyl ketone

: 34701-37-6
cyclohexylidene(phenyl)methyl acetate

Guidance literature:: With toluene-4-sulfonic acid; at 110 ℃; for 12h;
DOI:10.1002/ejoc.200390103

Reference yield:

: 95999-30-7
[cyclohexylidene(phenyl)methoxy]trimethylsilane

: 34701-37-6
cyclohexylidene(phenyl)methyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeLi / tetrahydrofuran / 1 h / 20 °C

1.2: CD₃COOD / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

2.1: 51 percent / p-TsOH / 12 h / 110 °C

With methyllithium; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1002/ejoc.200390103

Reference yield:

: 34701-37-6
cyclohexylidene(phenyl)methyl acetate

: 712-50-5
Cyclohexyl phenyl ketone

: 108954-06-9
[α-2H]cyclohexyl phenyl ketone

Guidance literature:: cyclohexylidene(phenyl)methyl acetate; In diethyl ether; at 20 ℃; for 1h;

With tetradeuterioacetic acid; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Title compound not separated from byproducts;
DOI:10.1002/ejoc.200390103