C₁₆H₁₃N₃O₄

Base Information

Chemical Name:C₁₆H₁₃N₃O₄
CAS No.:869791-95-7
Molecular Formula:C₁₆H₁₃N₃O₄
Molecular Weight:311.297
Hs Code.:

C<sub>16</sub>H<sub>13</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₃N₃O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₃N₃O₄

Chemical Property:

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Technology Process of C₁₆H₁₃N₃O₄

There total 5 articles about C₁₆H₁₃N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869791-94-6
C₁₅H₁₃N₃O₃

: 869791-95-7
C₁₆H₁₃N₃O₄

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 0 - 5 ℃; for 0.5h;

C₁₅H₁₃N₃O₃; In water; at 0 - 70 ℃;

Reference yield:

: 49787-37-3
1-acetyl-5-methoxy-indol-3-ol

: 869791-95-7
C₁₆H₁₃N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 2 h / Heating / reflux

2.1: triethylamine / methanol / Heating / reflux

3.1: trichlorophosphate / 0.5 h / 0 - 5 °C

3.2: 0 - 70 °C

With triethylamine; trichlorophosphate; toluene-4-sulfonic acid; In methanol; toluene; 3.1: Vilsmeier Formylation;

Reference yield:

: C₁₀H₉NO₅^(2-)*2Na⁽¹⁺⁾

: 869791-95-7
C₁₆H₁₃N₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyl acetate / 2 h / 70 °C

2.1: sodium sulfite / ethanol; water / 0.5 h / 75 °C / Heating / reflux

3.1: toluene-4-sulfonic acid / toluene / 2 h / Heating / reflux

4.1: triethylamine / methanol / Heating / reflux

5.1: trichlorophosphate / 0.5 h / 0 - 5 °C

5.2: 0 - 70 °C

With triethylamine; sodium sulfite; trichlorophosphate; toluene-4-sulfonic acid; In methanol; ethanol; water; ethyl acetate; toluene; 5.1: Vilsmeier Formylation;