Technology Process of C35H54N6O7Si
There total 6 articles about C35H54N6O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; sodium carbonate; XPhos;
In
water; N,N-dimethyl-formamide;
at 80 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; sodium carbonate; XPhos; 3-Carboxyphenylboronic acid / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere
2: N-chloro-succinimide / acetonitrile / 4 h / 20 °C
3: palladium diacetate; sodium carbonate; XPhos / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere
With
N-chloro-succinimide; 3-Carboxyphenylboronic acid; palladium diacetate; sodium carbonate; XPhos;
In
water; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / 0.5 h / 20 °C
1.2: 2 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 44 h / 85 - 90 °C
3.1: palladium diacetate; sodium carbonate; XPhos; 3-Carboxyphenylboronic acid / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere
4.1: N-chloro-succinimide / acetonitrile / 4 h / 20 °C
5.1: palladium diacetate; sodium carbonate; XPhos / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere
With
N-chloro-succinimide; 3-Carboxyphenylboronic acid; palladium diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; XPhos;
In
methanol; water; N,N-dimethyl-formamide; acetonitrile;