Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

Base Information

Chemical Name:Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester
CAS No.:107302-14-7
Molecular Formula:C₁₈H₂₅NO₇
Molecular Weight:367.399
Hs Code.:

Synonyms:Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

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Chemical Property of Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

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Technology Process of Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

There total 11 articles about Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 107302-13-6
(3R,4S)-4-Acetoxy-3-(2,2-dimethoxy-ethyl)-5-methyl-1,1-dioxo-3,4-dihydro-1H-1λ⁶-[1,2]thiazine-2-carboxylic acid benzyl ester

: 107302-14-7
Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

Guidance literature:: With ozone; In methanol; at -35 ℃; for 2h;
DOI:10.1021/jo00383a001

Reference yield:

: 107302-11-4
3-(2,2-Dimethoxy-ethyl)-5-methyl-1,1-dioxo-3,6-dihydro-1H-1λ⁶-[1,2]thiazine-2-carboxylic acid benzyl ester

: 107302-14-7
Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / CF₃CO₃H, K₂HPO₄ / CH₂Cl₂

2: 92 percent / KH / tetrahydrofuran

3: 1.) O₃; 2.) Me₂S

With dipotassium hydrogenphosphate; dimethylsulfide; trifluoroacetyl peroxide; potassium hydride; ozone; In tetrahydrofuran; dichloromethane;

Reference yield:

: 107302-08-9
sultam

: 107302-14-7
Acetic acid (1S,2S)-1-acetyl-2-benzyloxycarbonylamino-4,4-dimethoxy-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) AcOH, H₂O; 2.) PCC, alumina

2: methanolic HCl / methanol

3: 65 percent / CF₃CO₃H, K₂HPO₄ / CH₂Cl₂

4: 92 percent / KH / tetrahydrofuran

5: 1.) O₃; 2.) Me₂S

With hydrogenchloride; aluminum oxide; dipotassium hydrogenphosphate; dimethylsulfide; trifluoroacetyl peroxide; water; potassium hydride; ozone; acetic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;