acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester

Base Information

• Chemical Name: acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester
• CAS No.: 954424-32-9
• Molecular Formula: C₁₃H₁₆BrNO₄
• Molecular Weight: 330.178
• Mol file: 954424-32-9.mol

Synonyms:acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester

Chemical Property of acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester

There total 1 articles about acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1,3-diacetoxy-2-(4-aminophenyl)propane (131605-30-6) → acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester (954424-32-9)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester (954424-32-9) + 2-(cyclohex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (141091-37-4) → Acetic acid 3-acetoxy-2-(4-amino-3-cyclohex-1-enyl-phenyl)-propyl ester (954124-77-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene;

DOI:10.1016/j.bmcl.2010.05.013

upstream raw materials:

1,3-diacetoxy-2-(4-aminophenyl)propane

Downstream raw materials:

Acetic acid 3-acetoxy-2-(4-amino-3-cyclohex-1-enyl-phenyl)-propyl ester