C₃₈H₅₆N₄O₈Si

Base Information

Chemical Name:C₃₈H₅₆N₄O₈Si
CAS No.:1353660-67-9
Molecular Formula:C₃₈H₅₆N₄O₈Si
Molecular Weight:724.97
Hs Code.:

C<sub>38</sub>H<sub>56</sub>N<sub>4</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₅₆N₄O₈Si

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Chemical Property of C₃₈H₅₆N₄O₈Si

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Technology Process of C₃₈H₅₆N₄O₈Si

There total 6 articles about C₃₈H₅₆N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 873326-27-3
(R)-2-((S)-2-((tert-butoxycarbonyl)amino)-N-methyl propanamido)-3-(1H-indol-3-yl)propanoic acid

: 1353660-58-8
(2S,3S)-methyl 3-amino-3-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2-methoxypropanoate

: 1353660-67-9
C₃₈H₅₆N₄O₈Si

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-31-7
(E)-methyl 4-[tert-butyldimethylsilyloxymethyl]cinnamate

: 1353660-67-9
C₃₈H₅₆N₄O₈Si

Guidance literature:: Multi-step reaction with 5 steps

1: hydroquinidine 1 4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; water; potassium carbonate; potassium hydrogencarbonate; potassium hexacyanoferrate(III) / tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

2: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 23 h / -25 - 20 °C / Inert atmosphere

3: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

5: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

With hydroquinidine 1 4-phthalazinediyl diether; hydrogen azide; potassium dioxotetrahydroxoosmate(VI); methanesulfonamide; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; benzotriazol-1-ol; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; potassium hexacyanoferrate(III); diethylazodicarboxylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1: Sharpless dihydroxylation / 2: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-32-8
(2S,3R)-methyl 3-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,3-dihydroxypropanoate

: 1353660-67-9
C₃₈H₅₆N₄O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 23 h / -25 - 20 °C / Inert atmosphere

2: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

4: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

With hydrogen azide; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1002/chem.201101978