methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

Base Information

Chemical Name:methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate
CAS No.:92955-26-5
Molecular Formula:C₁₈H₁₉ClO₈
Molecular Weight:398.797
Hs Code.:

Synonyms:methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

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Technology Process of methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

There total 6 articles about methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 87907-09-3
methyl 3-O-benzyl-4-O-monochloroacetyl-β-L-idopyranuronate 1,2-(tert-butyl orthoacetate)

: 92955-26-5
methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

Guidance literature:: With pyridinium perchlorate; In 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(87)80268-9

Reference yield: 59.0%

: 87907-09-3
methyl 3-O-benzyl-4-O-monochloroacetyl-β-L-idopyranuronate 1,2-(tert-butyl orthoacetate)

: 87907-06-0
benzyl 6-O-acetyl-3-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranoside

: 87907-10-6
benzyl 6-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-chloroacetyl-α-L-idopyranosyluronate)-α-D-glucopyranoside

: 92955-26-5
methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

Guidance literature:: With 2,6-lutidinium perchlorate; In chlorobenzene; for 1.5h; Heating;
DOI:10.1016/0008-6215(84)85281-7

Reference yield: 35.0%

: 87907-09-3
methyl 3-O-benzyl-4-O-monochloroacetyl-β-L-idopyranuronate 1,2-(tert-butyl orthoacetate)

: 87907-10-6
benzyl 6-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-chloroacetyl-α-L-idopyranosyluronate)-α-D-glucopyranoside

: 92955-26-5
methyl 2-O-acetyl-1,5-anhydro-3-O-benzyl-4-O-chloroacetyl-xylo-hex-1-enitoluronate

Guidance literature:: With 2,6-lutidinium perchlorate; benzyl 6-O-acetyl-3-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranoside; In chlorobenzene; for 1.5h; Heating;
DOI:10.1016/0008-6215(84)85281-7