(6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

Base Information

Chemical Name:(6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol
CAS No.:144641-00-9
Molecular Formula:C₃₀H₅₂O₂
Molecular Weight:444.742
Hs Code.:

(6<i>E</i>,14<i>E</i>,18<i>E</i>)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

Synonyms:(6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

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Technology Process of (6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

There total 12 articles about (6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 111-02-4
2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene

: 144641-00-9,153650-82-9
(6E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,6,14,18,22-pentaene-10,11-diol

: 56882-08-7,144731-70-4
(10E,14E,18E)-2,6,10,15,19,23-hexamethyl-tetracosa-2,10,14,18,22-pentaene-6,7-diol

Guidance literature:: 2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1.5h;

With perchloric acid; In tetrahydrofuran; water; at 0 ℃; for 2.5h;
DOI:10.1021/ol3016836

Reference yield:

: 111-02-4
2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene

: 63976-65-8
(3R)-(6E,10E,14E,18E)-2,3-dihydroxy-2,3-dihydrosqualene

: 63976-64-7
(3S)-2,3-dihydroxy-2,3-dihydrosqualene

: 144641-00-9,153650-82-9
10(R),11(R)-Dihydroxy-10,11-dihydrosqualene

: 144731-70-4
6(R),7(R)-Dihydroxy-6,7-dihydrosqualene

Guidance literature:: With (3a,9R,3'''a,4'"b,9'"R)-9,9'-[1,4-phthalazinediylbis(oxy)]bis[6'-(methyloxy)-10,11-dihydrocinchonan]; osmium(VIII) oxide; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 24h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)74236-5

Reference yield:

: 111-02-4
2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene

: 63976-65-8
(3R)-(6E,10E,14E,18E)-2,3-dihydroxy-2,3-dihydrosqualene

: 144641-00-9,153650-82-9
10(R),11(R)-Dihydroxy-10,11-dihydrosqualene

: 144641-00-9,153650-82-9
10(S),11(S)-Dihydroxy-10,11-dihydrosqualene

: 144731-70-4
6(R),7(R)-Dihydroxy-6,7-dihydrosqualene

Guidance literature:: With (3a,9R,3'''a,4'"b,9'"R)-9,9'-[1,4-phthalazinediylbis(oxy)]bis[6'-(methyloxy)-10,11-dihydrocinchonan]; osmium(VIII) oxide; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 24h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)74236-5