(3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

Base Information

Chemical Name:(3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate
CAS No.:96555-56-5
Molecular Formula:C₂₀H₃₂O₅Si
Molecular Weight:380.557
Hs Code.:

Synonyms:(3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

Suppliers and Price of (3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

Chemical Property:

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Technology Process of (3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

There total 1 articles about (3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1445-91-6
(S)-1-phenylethanol

: 91424-40-7
3-(tert-butyldimethylsilyloxy)glutaric anhydride

: 109720-93-6
(R)-3-(tert-Butyl-dimethyl-silanyloxy)-pentanedioic acid methyl ester (S)-1-phenyl-ethyl ester

: 96555-56-5
(3S,1'S)-methyl 1'-phenylethyl 3-<(tert-butyldimethylsilyl)oxy>pentanedioate

: 109720-97-0
3-(tert-Butyl-dimethyl-silanyloxy)-pentanedioic acid bis-((R)-1-phenyl-ethyl) ester

Guidance literature:: With N,N-dimethylpyridine; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, -15 - 0 deg C, 9 h, 2.) Et₂O, 2.5 h;
DOI:10.1021/jm00393a030