(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

Base Information

Chemical Name:(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide
CAS No.:1268616-78-9
Molecular Formula:C₃₆H₄₆ClNO₄S
Molecular Weight:624.285
Hs Code.:

Synonyms:(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

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Chemical Property of (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

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Technology Process of (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

There total 1 articles about (1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 1268616-36-9
3,3-bis(3-phenylpropoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane

: 1268616-78-9
(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

Guidance literature:: N,N-dimethyl acetamide; With lithium diisopropyl amide; In tetrahydrofuran;

3,3-bis(3-phenylpropoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane; In tetrahydrofuran; at -65 ℃; for 2h;
DOI:10.1016/j.tet.2010.12.023

Reference yield: 76.0%

: 1268616-78-9
(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)-N,N-dimethylacetamide

: 1268616-80-3
[4,4-bis(3-phenylpropoxymethyl)cyclopent-1-enyl]-N,N-dimethylacetamide

Guidance literature:: With isopropylmagnesium chloride; In diethyl ether; toluene; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.023