methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

Base Information

Chemical Name:methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose
CAS No.:1333398-06-3
Molecular Formula:C₁₇H₂₂O₆
Molecular Weight:322.358
Hs Code.:

Synonyms:methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

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Technology Process of methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

There total 2 articles about methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1333398-03-0
methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-mannopyranoside

: 1333398-06-3
methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1016/j.tet.2011.07.014

Reference yield:

: 3162-96-7,4148-58-7,4153-17-7,4288-93-1,5328-47-2,6988-39-2,13566-32-0,14155-23-8,27994-50-9,37093-57-5,37093-59-7,57701-27-6,59168-66-0,64552-06-3,65391-13-1,65391-14-2,65530-26-9,66512-65-0,71117-36-7,71117-37-8,71117-41-4,72904-85-9,74560-56-8,79549-74-9,86783-81-5,96093-51-5,98633-13-7,110415-35-5,110415-36-6,110850-29-8,124020-29-7,126924-12-7,129263-21-4,131433-03-9,145920-49-6,146863-04-9
methyl-4,6-O-phenylmethylene-α-D-mannopyranoside

: 1333398-06-3
methyl 4,6-O-(R)-benzylidene-2-O-isopropyl-α-D-arabinohexopyranosid-3-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane / 3 h / 45 °C

2: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieve

With tetra(n-butyl)ammonium hydrogensulfate; pyridinium chlorochromate; sodium hydroxide; In dichloromethane;
DOI:10.1016/j.tet.2011.07.014