5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Base Information

Chemical Name:5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine
CAS No.:110522-21-9
Molecular Formula:C₂₉H₃₀N₂O₆
Molecular Weight:502.567
Hs Code.:

Synonyms:5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

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Chemical Property of 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

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Technology Process of 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

There total 3 articles about 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 110522-20-8
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

: 110522-21-9
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Guidance literature:: With sodium hydroxide; In methanol; for 4h; Ambient temperature;
DOI:10.1002/jhet.5570230609

Reference yield:

: 110522-18-4
Benzoic acid 2-[5-(3-benzyloxy-benzyl)-4-methoxy-2-oxo-2H-pyrimidin-1-ylmethoxy]-ethyl ester

: 110522-21-9
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 6N aq. HCl, H₂ / Pd/C / methanol / 1 h / 2206.5 Torr

2: 70 percent / potassium carbonate / dimethylformamide / 40 °C / overnight

3: 85 percent / aq. NaOH / methanol / 4 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570230609

Reference yield:

: 110522-19-5
5-(3-hydroxybenzyl)-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

: 110522-21-9
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-hydroxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / potassium carbonate / dimethylformamide / 40 °C / overnight

2: 85 percent / aq. NaOH / methanol / 4 h / Ambient temperature

With sodium hydroxide; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570230609