1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether

Base Information

• Chemical Name: 1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether
• CAS No.: 25096-42-8
• Molecular Formula: C₁₁H₁₈O₄
• Molecular Weight: 214.262

Synonyms:1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether

Chemical Property of 1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether

Chemical Property:

Purity/Quality:

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Technology Process of 1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether

There total 2 articles about 1-Ethoxycarbonyl-cyclohexen-⁽¹⁾-ol-⁽²⁾-methoxymethylaether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloromethyl methyl ether (107-30-2) + ethyl 2-oxocyclohexane carboxylate (1655-07-8) → 1-Ethoxycarbonyl-cyclohexen-(1)-ol-(2)-methoxymethylaether (25096-42-8)

Guidance literature:

Multistep reaction; (i) Na, (ii) /BRN= 505943/;

DOI:10.1016/S0040-4020(01)93011-X

Reference yield:

chloromethyl methyl ether (107-30-2) + ethyl 2-oxocyclohexane carboxylate (1655-07-8) → 1-methoxymethyl-2-oxo-cyclohexanecarboxylic acid ethyl ester (27334-56-1) + 1-Ethoxycarbonyl-cyclohexen-(1)-ol-(2)-methoxymethylaether (25096-42-8)

Guidance literature:

With diethyl ether; sodium;

DOI:10.1016/S0040-4020(01)93011-X DOI:10.1002/ardp.19582911106

Reference yield:

1-Ethoxycarbonyl-cyclohexen-(1)-ol-(2)-methoxymethylaether (25096-42-8) → ethyl cyclohexanecarboxylate (3289-28-9)

Guidance literature:

With ammonia; lithium; In diethyl ether;

DOI:10.1021/jo00833a027

upstream raw materials:

chloromethyl methyl ether

ethyl 2-oxocyclohexane carboxylate

Downstream raw materials:

ethyl cyclohexanecarboxylate

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