Technology Process of C26H26Cl2N4O4
There total 5 articles about C26H26Cl2N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3,5-dichloro-4-aminophenol; trichloromethyl chloroformate;
With
triethylamine;
In
ethyl acetate;
for 2h;
Heating / reflux;
C19H23N3O2;
In
chloroform; ethyl acetate;
for 19h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ammonium bicarbonate / palladium 10% on activated carbon / methanol / 5 h / Heating / reflux
2.1: triethylamine / ethyl acetate / 2 h / Heating / reflux
2.2: 19 h / Heating / reflux
With
ammonium bicarbonate; triethylamine;
palladium 10% on activated carbon;
In
methanol; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 20 °C
2.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
3.1: triethylamine / ethyl acetate / 2 h / Heating / reflux
3.2: 19 h / Heating / reflux
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
1,4-dioxane; dichloromethane; ethyl acetate;