N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

Base Information

Chemical Name:N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide
CAS No.:83626-66-8
Molecular Formula:C₂₈H₄₂N₄O₆S₄
Molecular Weight:658.929
Hs Code.:

Synonyms:N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

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Chemical Property of N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

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Technology Process of N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

There total 4 articles about N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6-(6-Amino-hexyldisulfanyl)-hexylamine; hydrobromide

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 83626-66-8
N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; at 50 ℃; for 20h;
DOI:10.1002/jps.2600710720

Reference yield:

: 24566-79-8
2-(6-bromohexyl)isoindole-1,3-dione

: 83626-66-8
N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium thiosulfate pentahydrate / methanol; H₂O / 1 h / Heating

2: iodine / methanol / 0.17 h / Heating

3: 78 percent / 48percent hydrobromic acid, propionic acid / 24 h / Heating

4: 72 percent / sodium bicarbonate / acetone; H₂O / 20 h / 50 °C

With hydrogen bromide; iodine; sodium hydrogencarbonate; sodium thiosulfate; propionic acid; In methanol; water; acetone;
DOI:10.1002/jps.2600710720

Reference yield:

: 83626-78-2
2,2'-[dithiobis(hexane-1,6-diyl)]bis[1H-isoindole-1,3(2H)-dione]

: 83626-66-8
N-(4-{6-[6-(4-Acetylamino-benzenesulfonylamino)-hexyldisulfanyl]-hexylsulfamoyl}-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 48percent hydrobromic acid, propionic acid / 24 h / Heating

2: 72 percent / sodium bicarbonate / acetone; H₂O / 20 h / 50 °C

With hydrogen bromide; sodium hydrogencarbonate; propionic acid; In water; acetone;
DOI:10.1002/jps.2600710720