1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID

Base Information

• Chemical Name: 1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID
• CAS No.: 1751-78-6
• Molecular Formula: C₁₂H₁₀N₂O₃
• Molecular Weight: 230.223
• Hs Code.: 2933990090
• Mol file: 1751-78-6.mol

Synonyms:1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID

Chemical Property of 1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID

Chemical Property:

• PSA: 82.19000
• LogP: 1.48080

Purity/Quality:

97% ^*data from raw suppliers

1-Oxo-2,3,4,9-tetrahydro-1h-pyrido-[3,4-B]indole-6-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID

There total 1 articles about 1-OXO-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE-6-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid ethyl ester (1967-75-5) → 1-oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid (1751-78-6)

Guidance literature:

With methanol; lithium hydroxide; water; at 90 ℃; for 2h;

Reference yield:

pentafluorophenyl trifloroacetate (14533-84-7) + 1-oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid (1751-78-6) → C18H9O3N2F5

Guidance literature:

With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2007.01.055

Reference yield:

1-oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid (1751-78-6) → C18H15N3O2

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dimethylformamide / 2 h / 20 °C

2: dimethylformamide / 80 °C

With pyridine; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2007.01.055

upstream raw materials:

1-oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid ethyl ester

Downstream raw materials:

1-Oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid [3-(4-phenyl-piperazin-1-yl)-propyl]-amide

1-Oxo-2,3,4,9-tetrahydro-1H-β-carboline-6-carboxylic acid {3-[4-(3-chloro-phenyl)-piperazin-1-yl]-propyl}-amide

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