15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside
CAS No.:1357000-60-2
Molecular Formula:C₅₉H₈₆INO₂₅
Molecular Weight:1336.23
Hs Code.:

15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Synonyms:15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Chemical Property of 15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Technology Process of 15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

There total 10 articles about 15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1357000-58-8
15-(p-iodophenyl)pentadecyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 1357000-53-3
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

: 1357000-60-2
15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -50 ℃; for 2.5h; Molecular sieve;
DOI:10.3987/COM-11-12332

Reference yield:

: 208986-22-5
15-(p-iodophenyl)pentadecanol

: 1357000-60-2
15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 2.5 h / -20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; triphenylphosphine / tetrahydrofuran / 1 h

3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -50 °C / Molecular sieve

With N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.3987/COM-11-12332

Reference yield:

: 1357000-56-6
15-(p-iodophenyl)pentadecyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

: 1357000-60-2
15-(p-iodophenyl)pentadecyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; triphenylphosphine / tetrahydrofuran / 1 h

2: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -50 °C / Molecular sieve

With N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; trifluorormethanesulfonic acid; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.3987/COM-11-12332