4-(TRIFLUOROMETHYL)PHENYLGLYOXAL HYDRATE

Base Information

• Chemical Name: 4-(TRIFLUOROMETHYL)PHENYLGLYOXAL HYDRATE
• CAS No.: 1736-56-7
• Molecular Formula: C9H5 F3 O2
• Molecular Weight: 202.133
• Hs Code.: 2914700090
• Mol file: 1736-56-7.mol

Synonyms:Glyoxal,(a,a,a-trifluoro-p-tolyl)- (7CI,8CI); 4-(Trifluoromethyl)phenylglyoxal

Chemical Property of 4-(TRIFLUOROMETHYL)PHENYLGLYOXAL HYDRATE

Chemical Property:

• Vapor Pressure: 0.0971mmHg at 25°C
• Melting Point: 83-85°C
• Boiling Point: 223.3°Cat760mmHg
• Flash Point: 84.1°C
• PSA: 57.53000
• Density: g/cm³
• LogP: 1.19880

Purity/Quality:

97% ^*data from raw suppliers

4-(Trifluoromethyl)phenylglyoxal ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(TRIFLUOROMETHYL)PHENYLGLYOXAL HYDRATE

There total 3 articles about 4-(TRIFLUOROMETHYL)PHENYLGLYOXAL HYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-(4-trifluoromethylphenyl)ethanone (709-63-7) → 4-trifluoromethylphenylglyoxal (1736-56-7)

Guidance literature:

With selenium (IV) oxide; In 1,4-dioxane; water; Heating;

DOI:10.1016/j.bmcl.2008.02.037

Reference yield:

2-bromo-1-[4-(trifluoromethyl)phenyl]ethanone (383-53-9) → 4-trifluoromethylphenylglyoxal (1736-56-7)

Guidance literature:

With dimethyl sulfoxide;

DOI:10.1021/jm00279a029

Reference yield:

α,α,α-trifluorotoluene (98-08-8) → 4-trifluoromethylphenylglyoxal (1736-56-7)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / CS₂

2: SeO₂

With aluminium trichloride; selenium(IV) oxide; In carbon disulfide;

DOI:10.1021/jm00342a035

upstream raw materials:

1-(4-trifluoromethylphenyl)ethanone

2-bromo-1-[4-(trifluoromethyl)phenyl]ethanone

α,α,α-trifluorotoluene

Downstream raw materials:

(6-methoxy-9H-pyrido[3,4-b]indol-1-yl)(4-(trifluoromethyl)phenyl)methanone

(9H-pyrido[3,4-b]indol-1-yl)(4-(trifluoromethyl)phenyl)methanone

N-(3-(benzyloxy)phenyl)-2-oxo-2-(4-(trifluoromethyl)phenyl)acetamide

N-(4-cyanophenyl)-2-oxo-2-(4-(trifluoromethyl)phenyl)acetamide