(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

Chemical Name:(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

CAS No.:88909-02-8
Molecular Formula:C₃₅H₄₂N₂O₅
Molecular Weight:570.729
Hs Code.:

(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo<a>quinolizine

Synonyms:(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

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Chemical Property of (+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzoquinolizine

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Technology Process of (+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine

There total 5 articles about (+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 61194-43-2
(+/-)-8-benzyloxy-2β-(6-benzyloxy-3,4-dihydro-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine

: 16531-04-7,61194-44-3
(+/-)-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-8-hydroxy-9,10-dimethoxy-2H-benzo quinolizine<(+/-)-alangicine>

: 88909-02-8
(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 19 - 30 ℃; for 2h;

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 88909-02-8
(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 7 h / 20 °C

2: 94 percent / PPE / CHCl₃ / 3 h / Heating

3: 48 percent / H₂ / 10percent Pd-C / ethanol / 2 h / 19 - 30 °C

With diethyl cyanophosphonate; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 56774-72-2,57130-35-5,109009-03-2
ethyl (+/-)-8-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine-2β-acetate

: 88909-02-8
(+/-)-8-benzyloxy-2β-(3,4-dihydro-6-hydroxy-7-methoxy-1-isoquinolyl)methyl-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9,10-dimethoxy-2H-benzo quinolizine

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 2 N aq. NaOH / ethanol / 24 h / 20 °C

2: 79 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 7 h / 20 °C

3: 94 percent / PPE / CHCl₃ / 3 h / Heating

4: 48 percent / H₂ / 10percent Pd-C / ethanol / 2 h / 19 - 30 °C

With sodium hydroxide; diethyl cyanophosphonate; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; chloroform; N,N-dimethyl-formamide;