2-Cyclohexylideneacetaldehyde

Base Information

• Chemical Name: 2-Cyclohexylideneacetaldehyde
• CAS No.: 1713-63-9
• Molecular Formula: C8H12 O
• Molecular Weight: 124.183
• Hs Code.: 2912299000
• DSSTox Substance ID: DTXSID40456047
• Nikkaji Number: J80.295F
• Mol file: 1713-63-9.mol

Synonyms:2-cyclohexylideneacetaldehyde;cyclohexylideneacetaldehyde;1713-63-9;Cyclohexyliden-acetaldehyd;cyclohexylidene acetaldehyde;2-cyclohexylidene-acetaldehyde;SCHEMBL1307852;DTXSID40456047;WJMVPTHPBIDWHB-UHFFFAOYSA-N;AKOS022504464;CS-0232205;EN300-126589;Z1251356876

Chemical Property of 2-Cyclohexylideneacetaldehyde

Chemical Property:

• PSA: 17.07000
• LogP: 2.07580
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 124.088815002
• Heavy Atom Count: 9
• Complexity: 117

Purity/Quality:

97% ^*data from raw suppliers

2-cyclohexylideneacetaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(=CC=O)CC1

Technology Process of 2-Cyclohexylideneacetaldehyde

There total 74 articles about 2-Cyclohexylideneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,2-tetramethylene-2-tosylpropanal (176313-05-6) → cyclohexylideneacetaldehyde (1713-63-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;

DOI:10.1016/S0040-4020(96)00072-5

Reference yield: 90.0%

2-Cyclohexylidene-N-methoxy-N-methyl-acetamide (124931-20-0) → cyclohexylideneacetaldehyde (1713-63-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1016/S0040-4039(01)80653-5

Reference yield: 86.0%

tris(ethoxyvinyl)borane (1151545-40-2) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → cyclohexylideneacetaldehyde (1713-63-9)

Guidance literature:

tris(ethoxyvinyl)borane; With diethylzinc; In toluene; at -78 ℃; for 0.333333h; Inert atmosphere;

cyclohexanone; In toluene; at -78 - 20 ℃; for 14h; Inert atmosphere;

With hydrogenchloride; water; In diethyl ether; toluene; at 0 ℃; pH=> 4; Inert atmosphere;

DOI:10.1021/ol9005757

upstream raw materials:

1-vinylcyclohexanol

1-allyl-1-cyclohexanol

2-cyclohexylidene ethanol

2-(cyclohex-1-en-1-yl)acetaldehyde

Downstream raw materials:

acetic acid-(2ξ-cyclohex-1-enyl-vinyl ester)

(+/-)-2-((E)-2-cyclohexyliden-ethylidene)-4-methoxy-cyclohexanone

1-cyclohex-1-enyl-2-cyclohexyliden-ethanol

cyclohexylideneacetic acid