1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

Base Information

Chemical Name:1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol
CAS No.:144221-90-9
Molecular Formula:C₂₈H₂₃NO₆
Molecular Weight:469.494
Hs Code.:

Synonyms:1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

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Chemical Property of 1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

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Technology Process of 1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

There total 3 articles about 1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 136773-81-4
Allyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-α-D-allopyranoside

: 136773-83-6
3-O-Benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranosyl trichloroacetimidate

: 144221-90-9
1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

: 136773-84-7
Allyl 3,6-di-O-benzyl-4-O-(3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranosyl)-2-deoxy-2-phthalimido-α-D-allopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1002/hlca.19920750505

Reference yield: 61.0%

: 136773-81-4
Allyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-α-D-allopyranoside

: 123212-53-3,129519-27-3,144300-02-7
Ethyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-1-thio-β-D-allopyranoside

: 144221-90-9
1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

: 136773-84-7
Allyl 3,6-di-O-benzyl-4-O-(3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranosyl)-2-deoxy-2-phthalimido-α-D-allopyranoside

Guidance literature:: With 4 A molecular sieve; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; for 6h; Ambient temperature;
DOI:10.1002/hlca.19920750505

Reference yield: 28.0%

: 136773-81-4
Allyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-α-D-allopyranoside

: 144221-80-7
1-O-Acetyl-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranose

: 144221-90-9
1,5-Anhydro-3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-D-ribo-hex-1-enitol

: 136773-84-7
Allyl 3,6-di-O-benzyl-4-O-(3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranosyl)-2-deoxy-2-phthalimido-α-D-allopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1002/hlca.19920750505