1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

Base Information

Chemical Name:1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril
CAS No.:131631-45-3
Molecular Formula:C₂₃H₂₇N₃O₃
Molecular Weight:393.486
Hs Code.:

Synonyms:1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

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Chemical Property of 1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

Chemical Property:

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Technology Process of 1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

There total 5 articles about 1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 176547-24-3
{3-Methoxy-4-[4-(2-oxo-3,4-dihydro-2H-quinolin-1-yl)-piperidine-1-carbonyl]-phenyl}-methyl-carbamic acid benzyl ester

: 131631-45-3
1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr;
DOI:10.1248/cpb.44.725

Reference yield:

: 160587-12-2
1-(piperidin-4-yl)-3,4-dihydroquinolin-2(1H)-one

: 131631-45-3
1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Et₃N, bis(2-oxo-3-oxazolydinyl)phosphinic chloride / CH₂Cl₂ / 1 h / Ambient temperature

2: 95 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr

With hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1248/cpb.44.725

Reference yield:

: 176547-21-0
4-(Benzyloxycarbonyl-methyl-amino)-2-methoxy-benzoic acid methyl ester

: 131631-45-3
1-[1-(2-Methoxy-4-methylaminobenzoyl)-4-piperidinyl]-3,4-dihydrocarbostyril

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / aq. NaOH / dioxane

2: 74 percent / Et₃N, bis(2-oxo-3-oxazolydinyl)phosphinic chloride / CH₂Cl₂ / 1 h / Ambient temperature

3: 95 percent / H₂ / 5percent Pd/C / ethanol / 760 Torr

With sodium hydroxide; hydrogen; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1248/cpb.44.725