Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester

Base Information

• Chemical Name: Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester
• CAS No.: 173681-60-2
• Molecular Formula: C₂₀H₁₅F₈IO₃
• Molecular Weight: 582.229

Synonyms:Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester

Chemical Property of Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester

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Technology Process of Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester

There total 4 articles about Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ³-benzo[d][1,2]iodoxol-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

peracetic acid (79-21-0) + 1-(4-tert-Butyl-2-iodo-phenyl)-2,2,2-trifluoro-1-pentafluorophenyl-ethanol (173681-59-9) → Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ3-benzo[d][1,2]iodoxol-1-yl ester (173681-60-2)

Guidance literature:

In acetic acid;

DOI:10.1016/0040-4039(95)01978-Q

Reference yield:

1-(4-(tertbutyl)phenyl)-2,2,2-trifluoroethanone (73471-97-3) → Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ3-benzo[d][1,2]iodoxol-1-yl ester (173681-60-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / 1.) mercury trifluoroacetate; 2.) I₂/NaI / 1.) 90 deg C, 5 d; 2.) CH₂Cl₂, RT, 5 d

2: 85 percent / -78 °C

3: 87 percent / acetic acid

With iodine; mercury(II) trifluoroacetate; sodium iodide; In acetic acid;

DOI:10.1016/0040-4039(95)01978-Q

Reference yield:

4-tert-butylmagnesium bromide (63488-10-8) → Acetic acid 6-tert-butyl-3-pentafluorophenyl-3-trifluoromethyl-3H-1λ3-benzo[d][1,2]iodoxol-1-yl ester (173681-60-2)

Guidance literature:

Multi-step reaction with 4 steps

2: 80 percent / 1.) mercury trifluoroacetate; 2.) I₂/NaI / 1.) 90 deg C, 5 d; 2.) CH₂Cl₂, RT, 5 d

3: 85 percent / -78 °C

4: 87 percent / acetic acid

With iodine; mercury(II) trifluoroacetate; sodium iodide; In acetic acid;

DOI:10.1016/0040-4039(95)01978-Q

upstream raw materials:

peracetic acid

1-(4-tert-Butyl-2-iodo-phenyl)-2,2,2-trifluoro-1-pentafluorophenyl-ethanol

1-(4-(tertbutyl)phenyl)-2,2,2-trifluoroethanone

4-tert-butylmagnesium bromide

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