C₃₄H₄₂F₃N₅O₉

Base Information

Chemical Name:C₃₄H₄₂F₃N₅O₉
CAS No.:1370251-30-1
Molecular Formula:C₃₄H₄₂F₃N₅O₉
Molecular Weight:721.731
Hs Code.:

C<sub>34</sub>H<sub>42</sub>F<sub>3</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₃₄H₄₂F₃N₅O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₂F₃N₅O₉

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Technology Process of C₃₄H₄₂F₃N₅O₉

There total 10 articles about C₃₄H₄₂F₃N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1355242-78-2
C₃₆H₄₁F₆N₅O₁₀

: 1370251-30-1
C₃₄H₄₂F₃N₅O₉

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/ja2104679

Reference yield:

: 1355242-72-6
C₂₀H₂₅NO₇

: 1370251-30-1
C₃₄H₄₂F₃N₅O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / methanol / 0.17 h / 20 °C

1.2: 2 h / 20 °C

2.1: copper(II) sulfate; sodium L-ascorbate / methanol; water

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C

4.1: lithium perchlorate / acetonitrile / 20 h / 70 °C

5.1: triethylamine / dichloromethane / 20 h

6.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h

7.1: triethylamine / dichloromethane / 20 h

8.1: potassium hydroxide / tetrahydrofuran / 0.25 h / 0 °C

With palladium 10% on activated carbon; hydrogen; lithium perchlorate; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja2104679

Reference yield:

: 1355242-71-5
C₂₁H₂₅NO₆

: 1370251-30-1
C₃₄H₄₂F₃N₅O₉

Guidance literature:: Multi-step reaction with 7 steps

1: copper(II) sulfate; sodium L-ascorbate / methanol; water

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C

3: lithium perchlorate / acetonitrile / 20 h / 70 °C

4: triethylamine / dichloromethane / 20 h

5: palladium 10% on activated carbon; hydrogen / methanol / 5 h

6: triethylamine / dichloromethane / 20 h

7: potassium hydroxide / tetrahydrofuran / 0.25 h / 0 °C

With palladium 10% on activated carbon; hydrogen; lithium perchlorate; copper(II) sulfate; sodium L-ascorbate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja2104679