Technology Process of C18H24O5
There total 10 articles about C18H24O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; potassium permanganate;
In
methanol;
Yield given;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / CSA / tetrahydrofuran / 45 h / Ambient temperature
2: 97 percent / KH, 18-crown-6 / tetrahydrofuran / 5 h / Ambient temperature
3: t-BuOK / dimethylsulfoxide / 0.33 h / 100 °C
4: 4percent aq. KMnO4, 0.5 N NaOH / methanol
With
sodium hydroxide; potassium permanganate; 18-crown-6 ether; camphor-10-sulfonic acid; potassium tert-butylate; potassium hydride;
In
tetrahydrofuran; methanol; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 95 percent / 2 N H2SO4 / methanol / 20 h / Ambient temperature
2: 89 percent / DMAP / CH2Cl2; pyridine / 96 h / Ambient temperature
3: 86 percent / LiAlH4 / tetrahydrofuran / 8 h / Ambient temperature
4: 87 percent / 2 N H2SO4 / tetrahydrofuran / 44 h / 60 °C
5: 80 percent / CSA / tetrahydrofuran / 45 h / Ambient temperature
6: 97 percent / KH, 18-crown-6 / tetrahydrofuran / 5 h / Ambient temperature
7: t-BuOK / dimethylsulfoxide / 0.33 h / 100 °C
8: 4percent aq. KMnO4, 0.5 N NaOH / methanol
With
dmap; sodium hydroxide; potassium permanganate; lithium aluminium tetrahydride; 18-crown-6 ether; sulfuric acid; camphor-10-sulfonic acid; potassium tert-butylate; potassium hydride;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; dimethyl sulfoxide;
