O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate

Base Information

• Chemical Name: O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate
• CAS No.: 123826-48-2
• Molecular Formula: C₈₈H₈₇Cl₄NO₂₀
• Molecular Weight: 1620.47

Synonyms:O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property of O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate

There total 1 articles about O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranose (123826-58-4) + trichloroacetonitrile (545-06-2) → O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate (123826-48-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; at -20 ℃; for 2.5h;

DOI:10.1016/0008-6215(89)85173-0

Reference yield: 87.0%

tributyl(methylthio)stannane (17314-32-8) + O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate (123826-48-2) → methyl O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-1-thio-α-D-mannopyranoside (123826-59-5)

Guidance literature:

With 3 A molecular sieve; boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at -20 ℃; for 2h;

DOI:10.1016/0008-6215(89)85173-0

Reference yield: 87.0%

methyl O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-1-thio-α-D-mannopyranoside (123826-49-3) + O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate (123826-48-2) → C171H173ClO37S (123826-60-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate;

DOI:10.1016/S0040-4039(00)72734-1

upstream raw materials:

O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranose

trichloroacetonitrile

Downstream raw materials:

methyl O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-1-thio-α-D-mannopyranoside

C₁₇₁H₁₇₃ClO₃₇S

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 123826-48-2 O-(3,6-di-O-benzyl-4-O-chloroacetyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-O-p-methylbenzoyl-α-D-mannopyranosyl trichloroacetimidate

Send

Send

Metric Ton KG G Pound L ML

Send

Send