3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

Base Information

Chemical Name:3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide
CAS No.:640278-13-3
Molecular Formula:C₁₆H₁₃Cl₃N₂O₄S
Molecular Weight:435.715
Hs Code.:

3-oxo-3-(toluene-4-sulfonylamino)-<i>N</i>-(2,4,6-trichloro-phenyl)-propionamide

Synonyms:3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

Chemical Property:

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Technology Process of 3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

There total 1 articles about 3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 634-93-5
2,4,6-trichloroaniline

: 145909-27-9
malonic acid monotosylamide

: 640278-13-3
3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; at 20 ℃;
DOI:10.1023/A:1023756005530

Reference yield: 83.0%

: 640278-13-3
3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

: sodium; 5-[hydroxy-(2,4,6-trichloro-phenylimino)-methyl]-3-(toluene-4-sulfonyl)-3H-[1,2,3]triazol-4-olate

Guidance literature:: With phenylsulfonyl azide; sodium ethanolate; In ethanol; at 20 ℃; for 24h;
DOI:10.1023/A:1023756005530

Reference yield:

: 640278-13-3
3-oxo-3-(toluene-4-sulfonylamino)-N-(2,4,6-trichloro-phenyl)-propionamide

: C₁₆H₉Cl₃N₄O₄S^(2-)*2Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NaOEt; benzenesulfonyl azide / ethanol / 24 h / 20 °C

2: H₂O / Heating

With phenylsulfonyl azide; sodium ethanolate; In ethanol; water;
DOI:10.1023/A:1023756005530