5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

Base Information

Chemical Name:5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane
CAS No.:1589037-86-4
Molecular Formula:C₂₂H₂₀BF₃O₂
Molecular Weight:384.206
Hs Code.:

Synonyms:5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

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Chemical Property of 5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

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Technology Process of 5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

There total 2 articles about 5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1589038-19-6
N-methyl-N-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)acetamide

: 201733-56-4
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

: 1589037-86-4
5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; C₉H₁₁I*ClH; sodium t-butanolate; In toluene; at 160 ℃; for 20h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1021/ja501649a

Reference yield:

: 1589038-36-7
N-(6-bromonaphthalen-2-yl)-N-methylacetamide

: 1423-27-4
2-(trifluoromethyl)phenylboronic acid

: 1589037-86-4
5,5-dimethyl-2-(6-(2-(trifluoromethyl)phenyl)naphthalen-2-yl)-1,3,2-dioxaborinane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 3 h / Reflux

2: sodium t-butanolate; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; C₉H₁₁I*ClH / toluene / 20 h / 160 °C / Inert atmosphere; Glovebox; Sealed tube

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; C₉H₁₁I*ClH; potassium carbonate; sodium t-butanolate; In ethanol; water; toluene;
DOI:10.1021/ja501649a