(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

Base Information

Chemical Name:(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester
CAS No.:113778-83-9
Molecular Formula:C₁₉H₂₈O₅
Molecular Weight:336.428
Hs Code.:

Synonyms:(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

Chemical Property:

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Technology Process of (5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

There total 4 articles about (5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 113778-57-7
3-phenylpropyl 7-hydroxy-3,5-dioxo-8-methylnonanoate

: 113778-83-9
(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

: 113830-19-6
3-phenylpropyl (3R^*,5S^*,7S^*)-3,5,7-trihydroxy-8-methylnonanoate

: 113830-18-5
3-phenylpropyl (3S^*,5R^*,7S^*)-3,5,7-trihydroxy-8-methylnonanoate

: 113778-58-8
3-phenylpropyl (3R^*,5R^*,7S^*)-3,5,7-trihydroxy-8-methylnonanoate

Guidance literature:: With tetramethylammonium triacetoxyborohydride; In acetic acid; for 0.5h; Further byproducts given; Ambient temperature;
DOI:10.1021/ja00219a035

Reference yield:

: 122-97-4
3-Phenyl-1-propanol

: 113778-83-9
(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / triethylamine / CH₂Cl₂ / 3.33 h / 40 °C

2: 35 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / Ambient temperature

3: 55 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / 0.02 h / -78 °C

4: 35 percent / tetramethylammonium triacetoxyborohydride / acetic acid / 0.5 h / Ambient temperature

With n-butyllithium; triethylamine; diisopropylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; hexane; dichloromethane; acetic acid;
DOI:10.1021/ja00219a035

Reference yield:

: 113778-34-0
3-phenylpropyl-3-oxo butanoate

: 113778-83-9
(5S,7S)-5,7-Dihydroxy-8-methyl-3-oxo-nonanoic acid 3-phenyl-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / Ambient temperature

2: 55 percent / diisopropylamine, n-butyllithium / tetrahydrofuran; hexane / 0.02 h / -78 °C

3: 35 percent / tetramethylammonium triacetoxyborohydride / acetic acid / 0.5 h / Ambient temperature

With n-butyllithium; diisopropylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; hexane; acetic acid;
DOI:10.1021/ja00219a035