N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

Base Information

Chemical Name:N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine
CAS No.:1233946-48-9
Molecular Formula:C₃₆H₃₆N₈O₅
Molecular Weight:660.732
Hs Code.:

N<sub>6</sub>-{2-[N<sub>1</sub>-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

Synonyms:N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

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Chemical Property of N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

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Technology Process of N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

There total 1 articles about N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1233946-47-8
3',5'-di-O-acetyl-N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

: 1233946-48-9
N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 24h;
DOI:10.1039/b9nj00705a

Reference yield: 63.0%

: 1233946-48-9
N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1233946-56-9
5'-O-(4,4'-dimethoxytrityl)-N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1039/b9nj00705a

Reference yield:

: 1233946-48-9
N₆-{2-[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

: 1233946-60-5
3'-O-(2-cyanoethyl-N,N-diisopropylaminophosphinoxy)-5'-O-(4,4'-dimethoxytrityl)-N₆-{2[N₁-(4-methoxytrityl)-imidazol-4-yl]ethylaminocarbonyl}-2'-deoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/b9nj00705a