2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

Base Information

Chemical Name:2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine
CAS No.:1334484-29-5
Molecular Formula:C₂₃H₂₈FNO₄S
Molecular Weight:433.544
Hs Code.:

Synonyms:2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

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Chemical Property of 2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

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Technology Process of 2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

There total 4 articles about 2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1334484-60-4
C₂₃H₂₈FNO₂S

: 1334484-29-5
2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja207944c

Reference yield:

: 1334484-59-1
C₁₈H₂₆O₂S

: 1334484-29-5
2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / Inert atmosphere

1.2: Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ja207944c

Reference yield:

: 25825-48-3
5-(3,3-dimethyloxiran-2-yl)-3-methylpentanal

: 1334484-29-5
2-fluoro-6-(7-(3,3-dimethyloxiran-2-yl)-5-methyl-2-(phenylsulfonyl)hept-1-en-3-yloxy)pyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / Inert atmosphere

2.2: Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ja207944c