allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

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Chemical Name:allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside
CAS No.:1042225-11-5
Molecular Formula:C₇₅H₆₇NO₂₄
Molecular Weight:1366.35
Hs Code.:

allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

Synonyms:allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

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Chemical Property of allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

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Technology Process of allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

There total 1 articles about allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1042225-10-4
C₅₄H₄₅Cl₃N₂O₁₈

: 286476-62-8
allyl 2,4-di-O-benzoyl-α-L-fucopyranoside

: 1042225-11-5
allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

Guidance literature:: C₅₄H₄₅Cl₃N₂O₁₈; allyl 2,4-di-O-benzoyl-α-L-fucopyranoside; In dichloromethane; at 20 ℃; for 0.75h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1039/b802235f

Reference yield:

: 1042225-11-5
allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

: 108-24-7
acetic anhydride

: 1042225-13-7
C₃₂H₄₃NO₁₉

Guidance literature:: allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside; With lithium hydroxide; In water; acetonitrile; for 1h;

With methylamine; In ethanol; for 120h;

acetic anhydride; In methanol; at 0 ℃; for 3h;
DOI:10.1039/b802235f

Reference yield:

: 1042225-11-5
allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside

: 64-19-7,77671-22-8
acetic acid

: C₇₅H₇₁NO₂₄

Guidance literature:: allyl 2,3-di-O-benzoyl-4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-fucopyranoside; With sodium tetrahydroborate; In water; isopropyl alcohol;

acetic acid; at 80 ℃; for 5h; pH=5;
DOI:10.1039/b802235f