3-Nitromesidine

Base Information

• Chemical Name: 3-Nitromesidine
• CAS No.: 1521-60-4
• Molecular Formula: C9H12 N2 O2
• Molecular Weight: 180.206
• Hs Code.: 2921430090
• Mol file: 1521-60-4.mol

Synonyms:Aniline,2,4,6-trimethyl-3-nitro- (6CI,7CI,8CI); Nitromesidine

Chemical Property of 3-Nitromesidine

Chemical Property:

• PSA: 71.84000
• LogP: 3.20660

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Nitromesidine

There total 10 articles about 3-Nitromesidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,4,6-trimethylaniline (88-05-1) → 2,4,6-trimethyl-3-nitro-aniline (1521-60-4)

Guidance literature:

With sulfuric acid; nitric acid; at 0 - 20 ℃; for 2h;

DOI:10.1021/acs.orglett.9b04034

Reference yield:

N-(2,4,6-trimethyl-3-nitro-phenyl)-phthalimide → 2,4,6-trimethyl-3-nitro-aniline (1521-60-4) + benzene-1,2-dicarboxylic acid (88-99-3,73607-73-5)

Guidance literature:

Reference yield:

acetic acid-(2,4,6-trimethyl-3-nitro-anilide) (696621-31-5) → 2,4,6-trimethyl-3-nitro-aniline (1521-60-4)

Guidance literature:

With hydrogenchloride; at 150 - 160 ℃;

upstream raw materials:

2,4-dinitromesitylene

acetic acid-(2,4,6-trimethyl-3-nitro-anilide)

2,4,6-trimethylaniline

sulfuric acid

Downstream raw materials:

2-fluoro-1,3,5-trimethyl-4-nitro-benzene

2-chloro-1,3,5-trimethyl-4-nitrobenzene

2,4,6-trimethyl-3-nitro-benzonitrile

acetic acid-(2,4,6-trimethyl-3-nitro-anilide)