(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

Base Information

Chemical Name:(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride
CAS No.:551944-34-4
Molecular Formula:C₂₄H₂₇ClO₂
Molecular Weight:382.93
Hs Code.:

Synonyms:(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

Chemical Property:

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Technology Process of (1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

There total 8 articles about (1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 551944-18-4
(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carboxylic acid

: 551944-34-4
(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

Guidance literature:: With thionyl chloride; In 1,2-dichloro-ethane; Heating;
DOI:10.1016/j.bmcl.2005.03.100

Reference yield:

: 5947-49-9
podocarpic acid

: 551944-34-4
(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: MeOH / benzene

2: Cs₂CO₃ / dimethylformamide

3: t-BuOK / dimethylsulfoxide

4: thionyl chloride / 1,2-dichloro-ethane / Heating

With methanol; thionyl chloride; potassium tert-butylate; caesium carbonate; In dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.bmcl.2005.03.100

Reference yield:

: 4614-56-6
methyl podocarpate

: 551944-34-4
(1S,4aS,10aR)-6-(benzyloxy)-1,4a-dimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene-1-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: Cs₂CO₃ / dimethylformamide

2: t-BuOK / dimethylsulfoxide

3: thionyl chloride / 1,2-dichloro-ethane / Heating

With thionyl chloride; potassium tert-butylate; caesium carbonate; In dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.03.100