diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

Base Information

Chemical Name:diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate
CAS No.:1357009-93-8
Molecular Formula:C₁₅H₂₁N₄O₅PS
Molecular Weight:400.395
Hs Code.:

Synonyms:diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

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Chemical Property of diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

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Technology Process of diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

There total 1 articles about diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 79521-53-2,140151-17-3
diethyl [(E)-4-bromobut-2-en-1-yl]phosphonate

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1357009-93-8
diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

Guidance literature:: diethyl [(E)-4-bromobut-2-en-1-yl]phosphonate; 1-Phenyl-1H-tetrazole-5-thiol; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; for 12h; Inert atmosphere;

With ammonium molybdate; water; dihydrogen peroxide; In ethanol; for 12h; Inert atmosphere;
DOI:10.1021/ol203431e

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 1357009-93-8
diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

: diethyl [(2E,4Z,6E)-7-phenylhepta-2,4,6-trien-1-yl]phosphonate

: 1357010-05-9
diethyl [(2E,4E,6E)-7-phenylhepta-2,4,6-trien-1-yl]phosphonate

Guidance literature:: diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

(E)-3-phenylpropenal; In tetrahydrofuran; at -78 - 0 ℃; for 1.33333h; optical yield given as %de; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ol203431e

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1357009-93-8
diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate

: diethyl [(2E,4Z)-7-phenylhepta-2,4-dien-1-yl]phosphonate

: 1357009-99-4
diethyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]phosphonate

Guidance literature:: diethyl {(E)-4-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]but-2-en-1-yl}phosphonate; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

3-phenyl-propionaldehyde; In tetrahydrofuran; at -78 - 0 ℃; for 1.33333h; optical yield given as %de; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ol203431e