(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

Base Information

Chemical Name:(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid
CAS No.:957774-19-5
Molecular Formula:C₆H₆O₃S*C₅₇H₅₉NO₆
Molecular Weight:1012.28
Hs Code.:

Synonyms:(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

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Chemical Property of (1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

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Technology Process of (1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

There total 8 articles about (1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957774-10-6
(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-D-glucitol

: 98-11-3
benzenesulfonic acid

: 957774-19-5
(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

Guidance literature:: In methanol; at 20 ℃; for 0.25h;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 957774-19-5
(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

1.2: 0.25 h / -78 °C

2.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 1 h / 0 °C

3.1: hydrogenchloride / di-isopropyl ether; water; isopropyl alcohol / 2 h / 80 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0.55 h / 0 - 20 °C

5.1: hydrazine / methanol / 3 h / 60 °C

6.1: methanol / 0.25 h / 20 °C

With hydrogenchloride; triethylsilane; n-butyllithium; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; triphenylphosphine; hydrazine; In tetrahydrofuran; methanol; hexane; di-isopropyl ether; water; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

: C₅₉H₆₂O₈

: 957774-19-5
(1S)-1-[5-[4-(2-aminoethyl)benzyl]-2-(benzyloxy)-4-methylphenyl]-1,5-anhydro-2,3,4,6-tetra-O-benzyl-D-glucitol benzenesulfonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / di-isopropyl ether; water; isopropyl alcohol / 2 h / 80 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 0.55 h / 0 - 20 °C

3: hydrazine / methanol / 3 h / 60 °C

4: methanol / 0.25 h / 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; triphenylphosphine; hydrazine; In tetrahydrofuran; methanol; di-isopropyl ether; water; isopropyl alcohol; toluene;