Technology Process of 5-<3,5-bis(benzyloxyphenyl)>pentan-3-one
There total 8 articles about 5-<3,5-bis(benzyloxyphenyl)>pentan-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diethyl ether;
In
benzene;
for 1h;
Ambient temperature;
aq. hydrochloric acid, ethyl acetate, 16 h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 95 percent / thionyl chloride, pyridine / CH2Cl2 / 3 h / Ambient temperature
2: 88 percent / dimethylformamide / 7 h / Ambient temperature
3: 91 percent / 30percent aq. sodium hydroxide / methanol / 72 h / Heating
4: 95 percent / potassium carbonate / acetone / 3 h / Heating
5: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating
6: 85 percent / pyridine / CHCl3 / 3 h / 0 °C
7: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature
8: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; 1,2-dimethoxyethane; thionyl chloride; diethyl ether; potassium carbonate;
In
methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / potassium carbonate / acetone / 3 h / Heating
2: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating
3: 85 percent / pyridine / CHCl3 / 3 h / 0 °C
4: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature
5: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h
With
pyridine; lithium aluminium tetrahydride; 1,2-dimethoxyethane; diethyl ether; potassium carbonate;
In
diethyl ether; chloroform; dimethyl sulfoxide; acetone; benzene;
