Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester

Base Information

• Chemical Name: Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester
• CAS No.: 1026792-95-9
• Molecular Formula: C₁₀H₁₇ClO₄S
• Molecular Weight: 268.762
• Mol file: 1026792-95-9.mol

Synonyms:Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester

Chemical Property of Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester

There total 1 articles about Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-acetoxy-2,2-pentamethylene-1-propanethiocyanate (137384-50-0) → Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester (1026792-95-9)

Guidance literature:

With water; chlorine; for 1h;

DOI:10.1248/cpb.44.122

Reference yield: 67.0%

Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester (1026792-95-9) → 3-Acetoxy-2,2-pentamethylene-1-propanesulfonamide (137384-51-1)

Guidance literature:

With ammonia; In dichloromethane; for 1h;

DOI:10.1248/cpb.44.122

Reference yield:

Acetic acid 1-chlorosulfonylmethyl-cyclohexylmethyl ester (1026792-95-9) → 3-hydroxy-2,2-pentamethylene-1-propanesulfonamide (137384-39-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NH₃ gas / CH₂Cl₂ / 1 h

2: 61 percent / NaOCH₃ / methanol / 0.5 h / Ambient temperature

With ammonia; sodium methylate; In methanol; dichloromethane;

DOI:10.1248/cpb.44.122

upstream raw materials:

3-acetoxy-2,2-pentamethylene-1-propanethiocyanate

Downstream raw materials:

3-Acetoxy-2,2-pentamethylene-1-propanesulfonamide

3-hydroxy-2,2-pentamethylene-1-propanesulfonamide