Technology Process of C28H23ClN3O4(1-)*Na(1+)
There total 8 articles about C28H23ClN3O4(1-)*Na(1+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C
2.1: diphenyl phosphoryl azide; triethylamine / toluene / 80 °C
3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
3.2: pH 4.0
4.1: sodium hydroxide / methanol / 0.5 h / 20 °C
With
lithium hydroxide monohydrate; dimethylsulfide borane complex; diphenyl phosphoryl azide; water; triethylamine; sodium hydroxide; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole;
In
tetrahydrofuran; methanol; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diphenyl phosphoryl azide; triethylamine / toluene / 80 °C
2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
2.2: pH 4.0
3.1: sodium hydroxide / methanol / 0.5 h / 20 °C
With
lithium hydroxide monohydrate; diphenyl phosphoryl azide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; toluene;