Technology Process of 2-Ethylpiperidine hydrochloride
There total 2 articles about 2-Ethylpiperidine hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen;
In
methanol; water;
at 80 ℃;
for 18h;
under 45004.5 Torr;
Autoclave;
DOI:10.1002/ejoc.201900450
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / 3 h / 0 °C
1.2: 1.5 h / 20 °C
2.1: palladium 10% on activated carbon; hydrogenchloride; hydrogen / methanol; water / 18 h / 80 °C / 45004.5 Torr / Autoclave
With
hydrogenchloride; 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; methanol; water;
DOI:10.1002/ejoc.201900450